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Beilstein J. Org. Chem. 2014, 10, 2800–2808, doi:10.3762/bjoc.10.297
Graphical Abstract
Figure 1: Synthesis of [1]rotaxane by self-inclusion of a host–guest-linked molecule: a) short molecular leng...
Figure 2: Synthesis of an insulated molecule via flipping phenomenon.
Scheme 1: The synthetic route to the PMβ-CD based linked [3]rotaxane with a 5,15-di([1,1'-biphenyl]-4-yl)porp...
Figure 3: The aromatic region of the 1H NMR spectra of 5 at 25 °C: 1) CDCl3, 2) CD3OD, and 3) CD3OD:D2O 1:1.
Scheme 2: Selective synthesis of fixed [3]rotaxane by Suzuki cross-coupling reaction.
Scheme 3: The synthetic routes to precursor of PM β-CD based insulated oligothiophene.
Scheme 4: Synthesis of dibromohexa(para-phenylene) with two PMCDs 20.
Scheme 5: Synthesis of pseudo-linked [3]rotaxanes via double self-inclusion through flipping.
Figure 4: The aromatic region of the 1H NMR spectra of 5 at 25 °C: 1) CDCl3, 2) CD3OD, and CD3OD/D2O 1:1.
Figure 5: The aromatic region of the 1H NMR spectra of 20 at 25 °C: 1) CDCl3, 2) CD3OD, and CD3OD/D2O 1:1.
Scheme 6: Synthesis of fixed [3]rotaxane via complexation with rhodium porphyrin.
Figure 6: Partial ROESY NMR spectrum of 26 (400 MHz, CDCl3) showing the NOEs between aromatic protons of the ...